346 УДК 543.64, 543.544, 543.39 ИССЛЕДОВАНИЕ БИОЛОГИЧЕСКИ АКТИВНЫХ ГЛИКОЗИДОВ ПОЛУЧЕННЫХ СПИРТОВОЙ ВЫТЯЖКОЙ ИЗ НЕПАЛЬСКОГО САНДАЛОВОГО ДЕРЕВА OSYRIS WIGHTIANA (НЕТРАДИЦИОННОЕ НАЗВАНИЕ WALL EX WIGHT) Саджа Л. <...> From the genus Osyris, phenyl propanoid, benzyl alcohol, iridoid and megastigmane, were isolated from the butanolic fractions as the new source. <...> Syringin (1) belongs to phenyl propanoids and di-O-methylcrenatin (2) is benzyl alcohol derivative. <...> Here the detail reports of isolation and structure elucidation of megastigmanes, iridoid, benzyl alcohol and phenyl propanoid from the new source, O. wightiana, are presented. <...> Polyamide was further used for preparing sub-fractions. <...> The IR spectra of pure compounds were recorded by using JASCO A-320 spectrophotometre. 1H NMR and 13C NMR 300 and AMX-500 MHz instrument, while 13C NMR spectra were recorded at 100 and 125 MHz. 1H-NMR and 13C-NMR chemical shifts were reported here in δ (ppm) and coupling constant values (J) were measured in Hz. Multiplicities of carbon signals were determined by DEPT 90o and 135o experiments. 2D NMR spectra were recorded on a Bruker Avance AMX 500 NMR spectrometer. 1H NMR spectra were recorded on Bruker ACMass Spectrometry The EI MS spectra were recorded on mass spectrometer Varian MAT 312. <...> Five sub-fractions were obtained by gradual elution with increasing methanol in H2O/MeOH system. <...> The sub-fraction OB-52 (15 g, eluted with 5% to 10% of MeOH in H2O) and OB-53 (11 g, eluted with 10% to 20% MeOH in H2O) were further subjected to the polyamide column chromatography with CHCl3-MeOH as the solvent. 8-Epideoxyloganic acid (3) was obtained from the sub-fraction OB-52, on eluting through recycling HPLC (using L-80 column) at 1:1 MeOH: H2O solvent system. <...> Result and Discussion Spectral data of compounds 1-5 are given in the experimental section. <...> The spectral data of compounds were compared with the reported data for the identifi cation. <...> Phenyl propanoid The phenyl propanoid glycoside, syringin (1) was isolated as the crystalline needles (Fig. 1). <...> The mass spectrum showed its base peak at m/z 210.1 (C11H14O4) due to cleavage of glycoside <...>